1CKP
HUMAN CYCLIN DEPENDENT KINASE 2 COMPLEXED WITH THE INHIBITOR PURVALANOL B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-02-15 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 53.550, 71.350, 72.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.000 - 2.050 |
R-factor | 0.192 |
Rwork | 0.192 |
R-free | 0.26000 |
Structure solution method | OTHER |
Starting model (for MR) | 1hck |
RMSD bond length | 0.007 |
RMSD bond angle | 23.800 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CCP4 |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.000 | 2.110 |
High resolution limit [Å] | 2.050 | 2.050 |
Rmerge | 0.055 | 0.185 |
Number of reflections | 17655 | |
<I/σ(I)> | 13.3 | |
Completeness [%] | 98.7 | 91.6 |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.4 | pH 7.4 |