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1BDA

CATALYTIC DOMAIN OF HUMAN SINGLE CHAIN TISSUE PLASMINOGEN ACTIVATOR IN COMPLEX WITH DANSYL-EGR-CMK (DANSYL-GLU-GLY-ARG CHLOROMETHYL KETONE)

Experimental procedure
Source typeROTATING ANODE
Source detailsRIGAKU RUH2R
Temperature [K]290
Detector technologyIMAGE PLATE
Collection date1996-06-13
DetectorMARRESEARCH
Spacegroup nameP 21 21 21
Unit cell lengths43.990, 80.780, 159.160
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution7.000 - 3.350
R-factor0.2037

*

Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1rtf
RMSD bond length0.010
RMSD bond angle25.745

*

Data reduction softwareMOSFLM
Data scaling softwareROTAGR
Phasing softwareX-PLOR (3.851)
Refinement softwareX-PLOR (3.851)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]25.0003.180
High resolution limit [Å]3.1003.100
Rmerge0.1470.630
Total number of observations27265

*

Number of reflections9414
<I/σ(I)>3.61.2
Completeness [%]86.755.2
Redundancy2.91.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, sitting drop

*

8.223

*

pH 8.2
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein2.8 (mg/ml)
21dropacetate10 (mM)
31reservoiracetate0.1 (M)
41reservoir0.2 (M)
51reservoirmPEG60008 (%)
61reservoirmethane pentanediol4 (%)

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건을2024-03-27부터공개중

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