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1A0G

L201A MUTANT OF D-AMINO ACID AMINOTRANSFERASE COMPLEXED WITH PYRIDOXAMINE-5'-PHOSPHATE

Experimental procedure
Source typeROTATING ANODE
Source detailsRIGAKU RUH2R
Temperature [K]293
Detector technologyIMAGE PLATE
Collection date1996-05-29
DetectorRIGAKU
Spacegroup nameP 21 21 21
Unit cell lengths77.340, 91.760, 88.690
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 2.000
R-factor0.216
Rwork0.216
R-free0.26300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1daa
RMSD bond length0.009
RMSD bond angle23.800

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Data reduction softwarePROCESS
Data scaling softwarePROCESS
Phasing softwareX-PLOR (3.1)
Refinement softwareX-PLOR (3.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]88.6901.900
High resolution limit [Å]1.7901.790
Rmerge0.0900.356
Number of reflections48469
<I/σ(I)>7.51.58
Completeness [%]80.850.6
Redundancy4.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

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9drop solution was mixed with an equal volume of reservoir solution

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropD-alanine50 (mM)
21dropalpha-ketoglutartrate50 (mM)
31reservoirTris-HCl100 (mM)
41reservoirPEG335029-33 (%(w/v))
51reservoirsodium acetate300-700 (mM)
61reservoirsodium azide5 (mM)

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PDB entries from 2024-03-27

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