1GMV

Structure of UreE

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MPG/DESY, HAMBURG BEAMLINE BW6
Synchrotron site	MPG/DESY, HAMBURG
Beamline	BW6
Temperature [K]	100
Spacegroup name	P 21 21 21
Unit cell lengths	40.114, 80.415, 99.848
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	17.000 - 2.800
R-factor	0.2369
Rwork	0.237
R-free	0.31790
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.278
Refinement software	CNS (1.0)

Data quality characteristics

	Overall
Low resolution limit [Å]	17.000
High resolution limit [Å]	2.800
Rmerge	0.087
Number of reflections	8277
Completeness [%]	98.5
Redundancy	9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6.5		pH 6.50