1COA

THE EFFECT OF CAVITY CREATING MUTATIONS IN THE HYDROPHOBIC CORE OF CHYMOTRYPSIN INHIBITOR 2

Experimental procedure

Spacegroup name	P 6 2 2
Unit cell lengths	68.925, 68.925, 53.094
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	13.700 - 2.200
R-factor	0.171
RMSD bond length	0.020
RMSD bond angle	0.058
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.200 *	2.200 *
Rmerge	0.107 *
Number of reflections	35386 *
Completeness [%]	95.4 *	95.2 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	8 *	4-6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	ammonium sulfate	40 (%(w/v))	precipitant
2	1	reservoir	Tris-HCl	50 (mM)