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Yorodumi- PDB-453d: 5'-D(*CP*GP*CP*GP*AP*AP*TP*TP*CP*GP*CP*G)-3'-BENZIMIDAZOLE COMPLEX -
+Open data
-Basic information
Entry | Database: PDB / ID: 453d | ||||||||||||||||||
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Title | 5'-D(*CP*GP*CP*GP*AP*AP*TP*TP*CP*GP*CP*G)-3'-BENZIMIDAZOLE COMPLEX | ||||||||||||||||||
Components | DNA (5'-D(*Keywords | DNA / MINOR GROOVE BINDING | Function / homology | Chem-E96 / DNA / DNA (> 10) | Function and homology information Method | X-RAY DIFFRACTION / Resolution: 1.8 Å | Authors | Neidle, S. | Citation | Journal: J.Chem.Soc.,Chem.Commun. / Year: 1999 | Title: Symmetric bis-benzimidazoles, a new class of sequence-selective DNA-binding molecules Authors: Neidle, S. / Mann, J. / Rayner, E.J. / Baron, A. / Opoku-Boahen, Y. / Simpson, I.J. / Smith, N.J. / Fox, K.R. / Hartley, J.A. / Kelland, L.R. History |
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-Structure visualization
Structure viewer | Molecule: MolmilJmol/JSmol |
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-Downloads & links
-Download
PDBx/mmCIF format | 453d.cif.gz | 27.3 KB | Display | PDBx/mmCIF format |
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PDB format | pdb453d.ent.gz | 17.7 KB | Display | PDB format |
PDBx/mmJSON format | 453d.json.gz | Tree view | PDBx/mmJSON format | |
Others | Other downloads |
-Validation report
Arichive directory | https://data.pdbj.org/pub/pdb/validation_reports/53/453d ftp://data.pdbj.org/pub/pdb/validation_reports/53/453d | HTTPS FTP |
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-Related structure data
Similar structure data |
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-Links
-Assembly
Deposited unit |
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1 |
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Unit cell |
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-Components
#1: DNA chain | Mass: 3663.392 Da / Num. of mol.: 2 / Source method: obtained synthetically #2: Chemical | ChemComp-E96 / | #3: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: X-RAY DIFFRACTION / Number of used crystals: 1 |
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-Sample preparation
Crystal | Density Matthews: 2.18 Å3/Da / Density % sol: 43.68 % | ||||||||||||||||||||||||||||
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Crystal grow | Temperature: 286 K / Method: vapor diffusion, hanging drop / pH: 7 Details: pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 286K | ||||||||||||||||||||||||||||
Components of the solutions |
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-Data collection
Diffraction | Mean temperature: 100 K |
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Diffraction source | Source: ROTATING ANODE / Type: RIGAKU RU200 / Wavelength: 1.5418 |
Detector | Type: RIGAKU RAXIS IV / Detector: IMAGE PLATE / Date: Sep 15, 1997 / Details: YALE MIRROR |
Radiation | Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength: 1.5418 Å / Relative weight: 1 |
Reflection | Resolution: 1.8→8 Å / Num. all: 6380 / Num. obs: 6157 / % possible obs: 98 % / Observed criterion σ(F): 4 / Observed criterion σ(I): 2 / Rmerge(I) obs: 0.044 |
-Processing
Software |
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Refinement | Resolution: 1.8→8 Å / σ(F): 4
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Refinement step | Cycle: LAST / Resolution: 1.8→8 Å
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Refine LS restraints |
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