5EZL
Crystal Structure of Fab of parasite invasion inhibitory antibody c1 - monoclinic form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-06 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.000020 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 101.420, 108.900, 97.400 |
Unit cell angles | 90.00, 97.75, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.200 | 2.490 | |
High resolution limit [Å] | 2.430 | 10.870 | 2.430 |
Rmerge | 0.148 | 0.025 | 1.411 |
Rmeas | 0.176 | 0.030 | 1.666 |
Total number of observations | 133813 | ||
Number of reflections | 39274 | 455 | 2911 |
<I/σ(I)> | 7.77 | 31.45 | 0.99 |
Completeness [%] | 99.3 | 97.2 | 99.6 |
Redundancy | 3.4 | 3.5 | |
CC(1/2) | 0.992 | 0.999 | 0.313 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 295 | 0.1 M HEPES-NaOH pH 7.0, 20% PEG 8000 |