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- PDB-6gxl: The hit-and-return system enables efficient time-resolved serial ... -
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Open data
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Basic information
Entry | Database: PDB / ID: 6gxl | ||||||
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Title | The hit-and-return system enables efficient time-resolved serial synchrotron crystallography: RADDAM2 | ||||||
![]() | Fluoroacetate dehalogenase![]() | ||||||
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Function / homology | ![]() | ||||||
Biological species | ![]() ![]() | ||||||
Method | ![]() ![]() ![]() | ||||||
![]() | Schulz, E.C. / Mehrabi, P. / Mueller-Werkmeister, H. / Tellkamp, F. / Stuart, W. / Persch, E. / De Gasparo, R. / Diederich, F. / Pai, E.F. / Miller, R.J.D. | ||||||
![]() | ![]() Title: The hit-and-return system enables efficient time-resolved serial synchrotron crystallography. Authors: Schulz, E.C. / Mehrabi, P. / Muller-Werkmeister, H.M. / Tellkamp, F. / Jha, A. / Stuart, W. / Persch, E. / De Gasparo, R. / Diederich, F. / Pai, E.F. / Miller, R.J.D. | ||||||
History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 138.8 KB | Display | ![]() |
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PDB format | ![]() | 107.7 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Arichive directory | ![]() ![]() | HTTPS FTP |
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-Related structure data
Related structure data | ![]() 6fsxC ![]() 6gxdC ![]() 6gxfC ![]() 6gxhC ![]() 6gxtC ![]() 3r3uS S: Starting model for refinement C: citing same article ( |
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Similar structure data |
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Links
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Assembly
Deposited unit | ![]()
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Unit cell |
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Components
#1: Protein | ![]() Mass: 34073.660 Da / Num. of mol.: 2 Source method: isolated from a genetically manipulated source Source: (gene. exp.) ![]() ![]() Strain: CGA009 / Gene: RPA1163 / Production host: ![]() ![]() ![]() ![]() #2: Water | ChemComp-HOH / | ![]() |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 1.94 Å3/Da / Density % sol: 36.57 % |
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Crystal grow![]() | Temperature: 293 K / Method: batch mode Details: PEG 3350 18 - 20 % CaCl 200 mM TrisHCL 100 mM pH 8.5 |
-Data collection
Diffraction | Mean temperature: 293 K |
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Diffraction source | Source: ![]() ![]() ![]() |
Detector | Type: DECTRIS PILATUS 6M / Detector: PIXEL / Date: May 1, 2017 |
Radiation | Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength![]() |
Reflection | Resolution: 1.8→81.42 Å / Num. obs: 48210 / % possible obs: 99.9 % / Redundancy: 9.5 % / Net I/σ(I): 3 |
Reflection shell | Resolution: 1.8→1.83 Å |
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Processing
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Refinement | Method to determine structure![]() ![]() Starting model: 3r3u Resolution: 1.8→40.722 Å / SU ML: 0.25 / Cross valid method: FREE R-VALUE / σ(F): 4.84 / Phase error: 27.79
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Solvent computation | Shrinkage radii: 0.9 Å / VDW probe radii: 1.11 Å | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Refinement step | Cycle: LAST / Resolution: 1.8→40.722 Å
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Refine LS restraints |
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LS refinement shell |
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