A: Complement factor D B: Complement factor D C: Complement factor D D: Complement factor D E: Complement factor D F: Complement factor D hetero molecules
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 1 Å / Relative weight: 1
Reflection
Resolution: 2.25→83.05 Å / Num. obs: 83798 / % possible obs: 100 % / Redundancy: 6.14 % / Net I/σ(I): 10
Reflection shell
Resolution: 2.25→2.32 Å
-
Processing
Software
Name
Version
Classification
REFMAC
5.8.0189
refinement
XDS
datareduction
XSCALE
datascaling
PHASER
phasing
Refinement
Resolution: 2.25→71.76 Å / Cor.coef. Fo:Fc: 0.932 / Cor.coef. Fo:Fc free: 0.912 / SU B: 8.421 / SU ML: 0.19 / Cross valid method: THROUGHOUT / ESU R: 0.268 / ESU R Free: 0.205 / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.24388
4190
5 %
RANDOM
Rwork
0.21761
-
-
-
obs
0.21892
79605
99.95 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å