解像度: 2.501→49.185 Å / SU ML: 0.32 / 交差検証法: FREE R-VALUE / σ(F): 1.36 / 位相誤差: 25.42 詳細: NCS restraints have been used. TLS refinement has been performed. The assignment of ions and PEG molecules is tentative only and their coordination is perturbed due to the limited resolution ...詳細: NCS restraints have been used. TLS refinement has been performed. The assignment of ions and PEG molecules is tentative only and their coordination is perturbed due to the limited resolution (we have not restrained the protein-ion distances beyond the standard routines of the PHENIX software).