解像度: 2.598→48.134 Å / SU ML: 0.27 / 交差検証法: FREE R-VALUE / σ(F): 1.36 / 位相誤差: 20.61 / 立体化学のターゲット値: ML 詳細: Density for the third HSB copy was clearly observable at the third RBS and a copy was manually placed by superimposing an HA-HSB complex from within the model. The position of the manually ...詳細: Density for the third HSB copy was clearly observable at the third RBS and a copy was manually placed by superimposing an HA-HSB complex from within the model. The position of the manually placed copy was further optimized by rigid body fitting within the FO-FC map in COOT and rigid body refinement in Phenix. The model was refined through iterative rounds of model building in COOT and refinement in Phenix. Several regions of the third copy of HSB are poorly ordered. The final model contains regions of the protein with 2FO-FC density for backbone atoms at 1.0 sigma.
Rfactor
反射数
%反射
Rfree
0.2042
4710
5.01 %
Rwork
0.1728
-
-
obs
0.1744
94061
99.77 %
溶媒の処理
減衰半径: 0.9 Å / VDWプローブ半径: 1.11 Å / 溶媒モデル: FLAT BULK SOLVENT MODEL