Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 3.9 Å3/Da / Density % sol: 69 % / Description: NONE
Crystal grow
Temperature: 291 K / Method: vapor diffusion, hanging drop / pH: 8 Details: 6.3 MG/ML OF LYSINE MODIFIED (ETHYLATED) PROTEIN IN 50 MM TRIS PH 8.0, 500 MM NACL, 5% GLYCEROL, 20 MM MGCL2, 2 MM IMIDAZOLE, 1 MM AMPPCP, MIXED 1:1 WITH 2.2 M AMMONIUM SULFATE, HANGING DROP, 18C
Resolution: 2.95→64.33 Å / Cor.coef. Fo:Fc: 0.956 / Cor.coef. Fo:Fc free: 0.926 / SU B: 16.991 / SU ML: 0.307 / Cross valid method: THROUGHOUT / ESU R: 1.081 / ESU R Free: 0.383 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.2533
993
10 %
RANDOM
Rwork
0.18495
-
-
-
obs
0.1918
8980
93.15 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK