Type: RIGAKU RAXIS IV / Detector: IMAGE PLATE / Date: Dec 15, 2010
Radiation
Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 1.5418 Å / Relative weight: 1
Reflection
Redundancy: 4.6 % / Av σ(I) over netI: 4.6 / Number: 80520 / Rsym value: 0.085 / D res high: 1.6 Å / D res low: 22.672 Å / Num. obs: 17668 / % possible obs: 98.4
Diffraction reflection shell
Highest resolution (Å)
Lowest resolution (Å)
% possible obs (%)
ID
Rmerge(I) obs
Rsym value
Redundancy
5.06
22.67
98.7
1
0.073
0.073
4.2
3.58
5.06
100
1
0.072
0.072
4.6
2.92
3.58
100
1
0.077
0.077
4.7
2.53
2.92
100
1
0.077
0.077
4.7
2.26
2.53
99.8
1
0.083
0.083
4.7
2.07
2.26
99.4
1
0.093
0.093
4.7
1.91
2.07
99.1
1
0.119
0.119
4.7
1.79
1.91
98.6
1
0.157
0.157
4.7
1.69
1.79
97.8
1
0.222
0.222
4.6
1.6
1.69
94.3
1
0.298
0.298
4.1
Reflection
Resolution: 1.6→22.672 Å / Num. all: 17955 / Num. obs: 17668 / % possible obs: 98.4 % / Redundancy: 4.6 % / Biso Wilson estimate: 18.6 Å2 / Rmerge(I) obs: 0.085 / Rsym value: 0.085 / Net I/σ(I): 11.3
Reflection shell
Diffraction-ID: 1
Resolution (Å)
Redundancy (%)
Rmerge(I) obs
Mean I/σ(I) obs
Num. measured all
Num. unique all
Rsym value
% possible all
1.6-1.69
4.1
0.298
2.5
9776
2411
0.298
94.3
1.69-1.79
4.6
0.222
3.3
10996
2381
0.222
97.8
1.79-1.91
4.7
0.157
4.5
10457
2248
0.157
98.6
1.91-2.07
4.7
0.119
5.6
9941
2132
0.119
99.1
2.07-2.26
4.7
0.093
6.8
9190
1960
0.093
99.4
2.26-2.53
4.7
0.083
7.6
8456
1809
0.083
99.8
2.53-2.92
4.7
0.077
7.4
7563
1610
0.077
100
2.92-3.58
4.7
0.077
7.3
6383
1368
0.077
100
3.58-5.06
4.6
0.072
7.6
5029
1100
0.072
100
5.06-22.672
4.2
0.073
6.5
2729
649
0.073
98.7
-
Phasing
Phasing
Method: molecular replacement
Phasing MR
Rfactor: 53.89 / Model details: Phaser MODE: MR_AUTO
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