Mass: 3098.997 Da / Num. of mol.: 1 / Source method: obtained synthetically Details: ATL IS ALFA-L-LNA (ALFA-L-RIBO CONFIGURED LOCKED NUCLEIC ACID OR [ (1S, 3R, 4S, 7R)-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO[2. 2.1]HEPT-1-YL]METHYL DIHYDROGEN PHOSPHATE
#2: DNA chain
5- D(*GP*CP*AP*GP*AP*AP*GP*CP*AP*G) -3
Mass: 3103.057 Da / Num. of mol.: 1 / Source method: obtained synthetically
Sequence details
MODRES: 1GV6 ATL A 2() ALFA-L-LNA (ALFA-L-RIBO CONFIGURED LOCKED NUCLEIC ACID OR [ (1S,3R,4S,7R)-7- ...MODRES: 1GV6 ATL A 2() ALFA-L-LNA (ALFA-L-RIBO CONFIGURED LOCKED NUCLEIC ACID OR [ (1S,3R,4S,7R)-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO [2.2.1]HEPT-1-YL]METHYL DIHYDROGEN PHOSPHATE MODRES: 1GV6 ATL A 5() ALFA-L-LNA (ALFA-L-RIBO CONFIGURED LOCKED NUCLEIC ACID OR [ (1S,3R,4S,7R)-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO [2.2.1]HEPT-1-YL]METHYL DIHYDROGEN PHOSPHATE MODRES: 1GV6 ATL A 6() ALFA-L-LNA (ALFA-L-RIBO CONFIGURED LOCKED NUCLEIC ACID OR [ (1S,3R,4S,7R)-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO [2.2.1]HEPT-1-YL]METHYL DIHYDROGEN PHOSPHATE MODRES: 1GV6 ATL A 8() ALFA-L-LNA (ALFA-L-RIBO CONFIGURED LOCKED NUCLEIC ACID OR [ (1S,3R,4S,7R)-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO [2.2.1]HEPT-1-YL]METHYL DIHYDROGEN PHOSPHATE
-
Experimental details
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Experiment
Experiment
Method: SOLUTION NMR
NMR experiment
Conditions-ID
Experiment-ID
Solution-ID
Type
1
1
1
NOESY
1
2
1
DQF-COSY
1
3
1
TOCSY
NMR details
Text: THE STRUCTURE WAS DETERMINED USING 1H,1H- NOES FROM 100MS NOESY AND WATERGATE NOESY EXPERIMENTS. SUGAR TORSION RESTRAINTS WERE DERIVED BY ANALYSIS OF A DQF-COSY SPECTRUM
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Sample preparation
Sample conditions
Ionic strength: 0.01 M / pH: 7.0 / Pressure: 1 atm / Temperature: 298 K
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