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Open data
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Basic information
Entry | Database: PDB / ID: 1c9z | ||||||||||||||||||
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Title | D232-CGTACG | ||||||||||||||||||
![]() | 5'-D(*![]() ![]() ![]() ![]() ![]() Function / homology | Chem-232 / | ![]() ![]() Method | ![]() ![]() Williams, L.D. | ![]() ![]() Title: Effects of cationic charge on three-dimensional structures of intercalative complexes: structure of a bis-intercalated DNA complex solved by MAD phasing. Authors: Shui, X. / Peek, M.E. / Lipscomb, L.A. / Gao, Q. / Ogata, C. / Roques, B.P. / Garbay-Jaureguiberry, C. / Wilkinson, A.P. / Williams, L.D. History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 14.4 KB | Display | ![]() |
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PDB format | ![]() | 7.7 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Arichive directory | ![]() ![]() | HTTPS FTP |
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-Related structure data
Related structure data | |
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Similar structure data |
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Links
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Assembly
Deposited unit | ![]()
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1 | ![]()
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Unit cell |
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Components on special symmetry positions |
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Components
#1: DNA chain | Mass: 1809.217 Da / Num. of mol.: 1 / Source method: obtained synthetically / Details: SYNTHETIC |
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#2: Chemical | ChemComp-232 / |
-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 2.22 Å3/Da / Density % sol: 44.5 % | ||||||||||||||||||||||||||||||||||||||||||||||||
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Crystal grow![]() | Temperature: 300 K / Method: vapor diffusion, sitting drop / pH: 6 Details: MPD, SPERMINE, MAGNESIUM CHLORIDE, SODIUM CACODYLATE, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 300K | ||||||||||||||||||||||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS | ||||||||||||||||||||||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 300 K |
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Diffraction source | Source: ![]() |
Detector | Type: UCSD MARK II / Detector: AREA DETECTOR / Date: Sep 9, 1995 |
Radiation | Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength![]() |
Reflection | Resolution: 2.4→10 Å / Num. all: 5220 / Num. obs: 4698 / % possible obs: 91 % / Observed criterion σ(F): 2 / Observed criterion σ(I): 4 / Redundancy: 3.2 % / Biso Wilson estimate: 21 Å2 / Rmerge(I) obs: 0.051 / Net I/σ(I): 9.2 |
Reflection shell | Resolution: 2.4→2.51 Å / Redundancy: 4.2 % / Rmerge(I) obs: 0.06 / % possible all: 84 |
Reflection | *PLUS Num. all: 4698 / Num. obs: 744 / % possible obs: 91 % / Num. measured all: 5220 / Rmerge(I) obs: 0.0514 |
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Processing
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Refinement | Resolution: 2.4→10 Å / σ(F): 4 / σ(I): 2 / Stereochemistry target values: PARKINSON ET AL.
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Refinement step | Cycle: LAST / Resolution: 2.4→10 Å
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Software | *PLUS Name: ![]() | |||||||||||||||||||||||||
Refinement | *PLUS Highest resolution: 2.4 Å / Lowest resolution: 10 Å / Num. reflection obs: 731 / σ(F): 4 | |||||||||||||||||||||||||
Solvent computation | *PLUS | |||||||||||||||||||||||||
Displacement parameters | *PLUS | |||||||||||||||||||||||||
Refine LS restraints | *PLUS
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