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Structure paper

TitleFacile Fabrication of Protein-Macrocycle Frameworks.
Journal, issue, pagesJ. Am. Chem. Soc., Vol. 143, Page 1896-1907, Year 2021
Publish dateMay 26, 2020 (structure data deposition date)
AuthorsRamberg, K.O. / Engilberge, S. / Skorek, T. / Crowley, P.B.
External linksJ. Am. Chem. Soc. / PubMed:33470808
MethodsX-ray diffraction
Resolution1.124 - 1.6 Å
Structure data

PDB-6z5g:
The RSL - sulfonato-calix[8]arene complex, I23 form, citrate pH 4.0, solved by S-SAD
Method: X-RAY DIFFRACTION / Resolution: 1.278 Å

PDB-6z5m:
The RSL - sulfonato-calix[8]arene complex, I23 form, Gly-HCl pH 2.2
Method: X-RAY DIFFRACTION / Resolution: 1.6 Å

PDB-6z5p:
The RSL-R8 - sulfonato-calix[8]arene complex, P3 form, TRIS-HCl pH 8.5
Method: X-RAY DIFFRACTION / Resolution: 1.42 Å

PDB-6z5q:
The RSL - sulfonato-calix[8]arene complex, P3 form, acetate pH 4.0
Method: X-RAY DIFFRACTION / Resolution: 1.29 Å

PDB-6z5w:
The RSL - sulfonato-calix[8]arene complex, P213 form, MES pH 6.8
Method: X-RAY DIFFRACTION / Resolution: 1.187 Å

PDB-6z5x:
The RSL - sulfonato-calix[8]arene complex, P213 form, acetate pH 4.8
Method: X-RAY DIFFRACTION / Resolution: 1.14 Å

PDB-6z5z:
The RSL-R6 - sulfonato-calix[8]arene complex, P213 form, TRIS-HCl pH 8.5
Method: X-RAY DIFFRACTION / Resolution: 1.124 Å

PDB-6z60:
The RSL - sulfonato-calix[8]arene complex, P213 form, CAPS pH 9.5
Method: X-RAY DIFFRACTION / Resolution: 1.166 Å

PDB-6z62:
The RSL - sulfonato-calix[8]arene complex, P213 form, TRIS-HCl pH 8.5
Method: X-RAY DIFFRACTION / Resolution: 1.156 Å

PDB-7alf:
The dimethylated RSL - sulfonato-calix[8]arene complex, P3 form, acetate pH 4.0
Method: X-RAY DIFFRACTION / Resolution: 1.261 Å

PDB-7alg:
The RSLex - sulfonato-calix[8]arene complex, P3 form, acetate pH 4.0
Method: X-RAY DIFFRACTION / Resolution: 1.452 Å

Chemicals

ChemComp-GOL:
GLYCEROL / Glycerol

ChemComp-BDF:
beta-D-fructopyranose / Fructose

ChemComp-EVB:
sulfonato-calix[8]arene

ChemComp-HOH:
WATER / Water

ChemComp-SO4:
SULFATE ION / Sulfate

ChemComp-NA:
Unknown entry

Source
  • ralstonia solanacearum (bacteria)
KeywordsSUGAR BINDING PROTEIN / calixarene / protein framework / cage / crystal engineering / molecular glue / synthetic receptor / macrocycle / biomaterial / supercharged

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